May 22-27, 2016
Naturally occurring structural materials are composites with very high filling degrees on hard constituent. In recent years structure and properties of biological materials have been studied in detail. But it has not been possible to reconstruct this structural design. In this contribution we present a process for the fabrication of very highly filled composite materials by using of the spouted bed spray granulation process.
Spouted bed granulation offers many advantages for the design of composite materials. In this investigation fine particles (dP =10-50 µm) could be uniformly spouted, and optimal properties for further processing to bulk materials can be obtained by means of granulation. For this a hybrid spouted bed with horizontal gas inlets was designed, which has a small prismatic process chamber with adjustable inlets and a high conical-cylindrical relaxation zone. The thickness of the polymer layer is adjusted by a two-fluid nozzle. The adjustment of the thickness of polymer layer is very important to fabricate composites of adjustable filling degrees. After granulation the particles are assembled to a composite material by means of warm pressing. Additionally for achievement of very high packing densities bimodal particle size distributions are used. For this purpose, particles in nm-range are firstly suspended in polymer solution and the suspension is sprayed in the spouted bed on coarser particles. Granulated particles are assembled to composites and mechanical properties of these were analysed by 4-point bending-tests.
We gratefully acknowledge financial support from the German Research Foundation (DFG) via the collaborative research center SFB986.
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Eduard Eichner, V. Salikov, M. Dosta, S. Heinrich, and G.A. Schneider, "Using of spouted bed spray granulation process for fabricating of metal/ceramic-polymer composites" in "Fluidization XV", Jamal Chaouki, Ecole Polytechnique de Montreal, Canada Franco Berruti, Wewstern University, Canada Xiaotao Bi, UBC, Canada Ray Cocco, PSRI Inc. USA Eds, ECI Symposium Series, (2016). http://dc.engconfintl.org/fluidization_xv/107